[PDF] Handbook Of X Ray Crystallography eBook

Author : Yoshio Waseda
Publisher : Springer Science & Business Media
Page : 320 pages
File Size : 32,70 MB
Release : 2011-03-18
Category : Technology & Engineering
ISBN : 3642166350

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X-ray diffraction crystallography for powder samples is a well-established and widely used method. It is applied to materials characterization to reveal the atomic scale structure of various substances in a variety of states. The book deals with fundamental properties of X-rays, geometry analysis of crystals, X-ray scattering and diffraction in polycrystalline samples and its application to the determination of the crystal structure. The reciprocal lattice and integrated diffraction intensity from crystals and symmetry analysis of crystals are explained. To learn the method of X-ray diffraction crystallography well and to be able to cope with the given subject, a certain number of exercises is presented in the book to calculate specific values for typical examples. This is particularly important for beginners in X-ray diffraction crystallography. One aim of this book is to offer guidance to solving the problems of 90 typical substances. For further convenience, 100 supplementary exercises are also provided with solutions. Some essential points with basic equations are summarized in each chapter, together with some relevant physical constants and the atomic scattering factors of the elements.

Author : Sharon Levine
Publisher :
Page : 0 pages
File Size : 28,25 MB
Release : 2015-03-30
Category : X-ray crystallography
ISBN : 9781632382849

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X-ray Crystallography is a scientific technique used to demonstrate the arrangement of atoms of a crystalline solid in 3D space. This book is a collection of latest trends, using X-ray crystallography and related structural determination techniques in a diverse variety of spheres. The procedures emphasized in this book consist of various processes and spectroscopic complimentary methods. The spectrum ranges from basic organic compounds to metal complexes to proteins and includes meta-analyses of a host of weak connections.

Author : Li-ling Ooi
Publisher : Oxford University Press, USA
Page : 168 pages
File Size : 46,17 MB
Release : 2010
Category : Language Arts & Disciplines
ISBN : 0199569045

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"With an understanding of three-dimensional structure being so central to the understanding of molecular function, Principles of X-ray Crystallography is the perfect guide for anyone needing to gain a working insight into X-ray crystallography." --Book Jacket.

Author : Albrecht Messerschmidt
Publisher : John Wiley & Sons
Page : 318 pages
File Size : 11,53 MB
Release : 2007-02-27
Category : Science
ISBN : 3527609679

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Written by one of the most significant contributors to the progress of protein crystallography, this practical guide contains case studies, a troubleshooting section and pointers on data interpretation. It covers the theory, practice and latest achievements in x-ray crystallography, such that any researcher in structural biology will benefit from this extremely clearly written book. Part A covers the theoretical basis and such experimental techniques as principles of x-ray diffraction, solutions for the phase problem and time-resolved x-ray crystallography. Part B includes case studies for different kinds of x-ray crystal structure determination, such as the MIRAS and MAD techniques, molecular replacement, and the difference Fourier technique.

Author : Kari Rissanen
Publisher : Springer Science & Business Media
Page : 190 pages
File Size : 50,27 MB
Release : 2012-01-10
Category : Science
ISBN : 3642274072

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Computational Studies of Crystal Structure and Bonding, by Angelo Gavezzotti Cryo-Crystallography: Diffraction at Low Temperature and More, by Piero Macchi High-Pressure Crystallography, by Malcolm I. McMahon Chemical X-Ray Photodiffraction: Principles, Examples, and Perspectives, by Panče Naumov Powder Diffraction Crystallography of Molecular Solids, by Kenneth D. M. Harris

Author : Michael M. Woolfson
Publisher : Cambridge University Press
Page : 422 pages
File Size : 29,98 MB
Release : 1997-01-13
Category : Medical
ISBN : 9780521423595

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A textbook for the student beginning a serious study of X-ray crystallography.

Author : Myeongkyu Lee
Publisher : CRC Press
Page : 302 pages
File Size : 23,98 MB
Release : 2017-03-16
Category : Science
ISBN : 1315361973

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X-ray diffraction is a useful and powerful analysis technique for characterizing crystalline materials commonly employed in MSE, physics, and chemistry. This informative new book describes the principles of X-ray diffraction and its applications to materials characterization. It consists of three parts. The first deals with elementary crystallography and optics, which is essential for understanding the theory of X-ray diffraction discussed in the second section of the book. Part 2 describes how the X-ray diffraction can be applied for characterizing such various forms of materials as thin films, single crystals, and powders. The third section of the book covers applications of X-ray diffraction. The book presents a number of examples to help readers better comprehend the subject. X-Ray Diffraction for Materials Research: From Fundamentals to Applications also • provides background knowledge of diffraction to enable nonspecialists to become familiar with the topics • covers the practical applications as well as the underlying principle of X-ray diffraction • presents appropriate examples with answers to help readers understand the contents more easily • includes thin film characterization by X-ray diffraction with relevant experimental techniques • presents a huge number of elaborately drawn graphics to help illustrate the content The book will help readers (students and researchers in materials science, physics, and chemistry) understand crystallography and crystal structures, interference and diffraction, structural analysis of bulk materials, characterization of thin films, and nondestructive measurement of internal stress and phase transition. Diffraction is an optical phenomenon and thus can be better understood when it is explained with an optical approach, which has been neglected in other books. This book helps to fill that gap, providing information to convey the concept of X-ray diffraction and how it can be applied to the materials analysis. This book will be a valuable reference book for researchers in the field and will work well as a good introductory book of X-ray diffraction for students in materials science, physics, and chemistry.

Author : George H. Stout
Publisher : John Wiley & Sons
Page : 484 pages
File Size : 34,99 MB
Release : 1989-05-08
Category : Science
ISBN : 0471607118

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Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.

Author : Allen G. Jackson
Publisher : Springer Science & Business Media
Page : 224 pages
File Size : 29,80 MB
Release : 2012-12-06
Category : Science
ISBN : 1461230527

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This book resulted from a series of frustrations. Analytical electron microscopy requires exactly what its name implies: quantitative information to conduct an analysis. The frustrations arose when I started hunting for specific forms of equations in a form understandable to a non-crystaHographer, for definitions of subtle concepts related to crystallography, for intelligible interpretations of space group symbols and their significance. What I frequently discovered was that such information was buried in a giant tome and couched in terms familiar to crystallographers but not to electron microscopists in general, or it was located in an old reference not available in my library, or it was found in an out-of-print book, or it was in a Russian book no longer available, etc. So to minimize the frustrations, I started a notebook containing the details, particularly after I had found forms of equations useful for quick calculations or equations in a form useful for proving, doing, or extending calculations found in a reference. The resulting notebook grew to a respectable size, requiring some organizing of the contents. Finally, the size became large enough, and has proven useful enough, to produce the notebook as a book.