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Author : Ray Freeman
Publisher : Longman Publishing Group
Page : 368 pages
File Size : 45,36 MB
Release : 1997
Category : Science
ISBN :
This new edition has been thoroughly revised to bring the handbook up-to-date.
Author : Frank A. Bovey
Publisher : Elsevier
Page : 668 pages
File Size : 27,88 MB
Release : 1988-11-01
Category : Science
ISBN : 0080916996
Nuclear Magnetic Resonance Spectroscopy, Second Edition focuses on two-dimensional nuclear magnetic resonance (NMR) spectroscopy, high resolution NMR of solids, water suppression, multiple quantum spectroscopy, and NMR imaging. The selection first takes a look at the fundamental principles and experimental methods. Discussions focus on the NMR phenomenon, dipolar broadening and spin-spin relaxation, nuclear electric quadrupole relaxation, saturation, magnetic shielding and chemical shift, magnetic field, transitions between the nuclear energy levels, and resolution and sensitivity considerations. The manuscript then ponders on chemical shift, coupling of nuclear spins, and nuclear relaxation and chemical rate processes. Topics include spin lattice relaxation, spin-spin relaxation, spin decoupling and associated techniques, and description and analysis of spin systems. The text examines two-dimensional NMR spectroscopy, macromolecules, and NMR of solids, including magic angle spinning, cross polarization, proton dipolar broadening, biopolymers, and chain motion in macromolecules. The selection is a valuable source of data for readers interested in nuclear magnetic resonance spectroscopy.
Author : T.I. Atta-Ur-Rahman
Publisher : Springer Science & Business Media
Page : 366 pages
File Size : 21,8 MB
Release : 2012-12-06
Category : Science
ISBN : 1461248949
Nuclear magnetic resonance spectroscopy is presently going through an explosive phase of development. This has been brought about largely on account of the advent of Fourier transform NMR spectrometers linked to powerful microcomputers which have opened up a whole new world for structural chemists and biochemists. This is exemplified by a host of publications, especially on new pulse sequences, which continue to provide new exciting modifications for recording two-dimensional NMR. Moreover, NMR is no longer confined to structural chemists but has moved firmly into the area of medicine as a powerful nondestructive body scanning technique. With this background, I felt that there was need for a text which would provide a fairly comprehensive account of the important features of 1 H- and 13C-NMR spectroscopy in one book, as well as make available an up-to-date account of recent developments of new pulse sequences, with particular reference to 2D-NMR spectroscopy. Since this book is written for students of chemistry and biochemistry as well as for biology students who have chemistry as a subsidiary, it was decided to avoid a complex mathematical treatment and to present, as far as possible without oversimplification, a qualitative account of 1 H- and 13C-NMR spectroscopy as it is today. I hope that the book satisfactorily meets these objectives.
Author : Frank Alden Bovey
Publisher :
Page : 418 pages
File Size : 35,55 MB
Release : 1969
Category : Science
ISBN :
Nine chapters cover: fundamental principles; experimental methods; the chemical shift; coupling of nuclear spins; nuclear relaxation and chemical rate processes; two-dimensional nuclear magnetic resonance spectroscopy; macromolecules; NMR of solids; special topics. Annotation copyrighted by Book News, Inc., Portland, OR
Author : P. J. Hore
Publisher :
Page : 121 pages
File Size : 42,29 MB
Release : 2015
Category : Science
ISBN : 0198703414
Nuclear Magnetic Resonance offers an accessible introduction to the physical principles of liquid-state NMR, with examples, applications, and exercises provided throughout to enable beginning undergraduates to get to grips with this important analytical technique.
Author : L. M. Jackman
Publisher : Elsevier
Page : 474 pages
File Size : 38,24 MB
Release : 2013-10-22
Category : Science
ISBN : 1483280942
Application of Nuclear Magnetic Resonance Spectroscopy in Organic Chemistry, Second Edition covers the theoretical background necessary for the intelligent application of NMR spectroscopy to common problems encountered in organic chemistry. This book is composed of five parts, and begins with introduction to the theory and practice of nuclear magnetic resonance. The succeeding chapter deals with the theory of chemical effects in NMR spectroscopy. These topics are followed by a discussion on the application of chemical shift to organic compound analysis and the principles of the spin-spin coupling .The final chapter considers the applications of time- dependent phenomena in NMR spectroscopy. This book will prove useful to analytical chemists and researchers in the allied fields.
Author : Joseph B. Lambert
Publisher : John Wiley & Sons
Page : 485 pages
File Size : 30,73 MB
Release : 2019-01-04
Category : Science
ISBN : 1119295238
Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.
Author : United States. Federal Grain Inspection Service
Publisher :
Page : pages
File Size : 21,99 MB
Release : 2003
Category :
ISBN :
Author : Myer Kutz
Publisher : John Wiley & Sons
Page : 832 pages
File Size : 26,9 MB
Release : 2016-04-25
Category : Science
ISBN : 1118647246
A multidisciplinary reference of engineering measurement tools, techniques, and applications "When you can measure what you are speaking about, and express it in numbers, you know something about it; but when you cannot measure it, when you cannot express it in numbers, your knowledge is of a meager and unsatisfactory kind; it may be the beginning of knowledge, but you have scarcely in your thoughts advanced to the stage of science." — Lord Kelvin Measurement is at the heart of any engineering and scientific discipline and job function. Whether engineers and scientists are attempting to state requirements quantitatively and demonstrate compliance; to track progress and predict results; or to analyze costs and benefits, they must use the right tools and techniques to produce meaningful data. The Handbook of Measurement in Science and Engineering is the most comprehensive, up-to-date reference set on engineering and scientific measurements—beyond anything on the market today. Encyclopedic in scope, Volume 3 covers measurements in physics, electrical engineering and chemistry: Laser Measurement Techniques Magnetic Force Images using Capacitive Coupling Effect Scanning Tunneling Microscopy Measurement of Light and Color The Detection and Measurement of Ionizing Radiation Measuring Time and Comparing Clocks Laboratory-Based Gravity Measurement Cryogenic Measurements Temperature-Dependent Fluorescence Measurements Voltage and Current Transducers for Power Systems Electric Power and Energy Measurement Chemometrics for the Engineering and Measurement Sciences Liquid Chromatography Mass Spectroscopy Measurements of Nitrotyrosine-Containing Proteins Fluorescence Spectroscopy X-Ray Absorption Spectroscopy Nuclear Magnetic Resonance (NMR) Spectroscopy Near Infrared (NIR) Spectroscopy Nanomaterials Properties Chemical Sensing Vital for engineers, scientists, and technical managers in industry and government, Handbook of Measurement in Science and Engineering will also prove ideal for academics and researchers at universities and laboratories.
Author : Robert A. Izydore
Publisher : Durham Eagle Publications
Page : 252 pages
File Size : 44,29 MB
Release : 2007
Category : Science
ISBN : 9780979843402
Nuclear magnetic resonance (NMR) spectroscopy is arguably the most important analytical tool that is that is available to chemists. It can be used to determine structures of molecules, study reaction mechanisms and reaction kinetics, and measure molecular properties. "Fundamentals of Nuclear Magnetic Resonance Spectroscopy" presents the fundamental concepts and applications of NMR spectroscopy. The book was written for advanced undergraduate and graduate students as well as for professional chemists. Highlights include . NMR theory and applications . NMR instrumentation . Relaxation processes, relaxation time determination, relaxation time applications . Chapters on 1H, 13C, 15N, and 2D-NMR . Exercises at the end of each chapter . Chapter of NMR exercises . Research applications in each chapter . Discussion and examples of DEPT, HET-2DJ, HOM-2DJ, HOM-COR/COSY, HET-COR, HMQC, HMBC, 2D-INADEQUATE, NOE difference, NOESY, ROESY, and TOSCY spectra