[PDF] Measurement Of Particle Size And Shape By Laser Light Scattering eBook

Author : Henk G. Merkus
Publisher : Springer Science & Business Media
Page : 535 pages
File Size : 39,99 MB
Release : 2009-01-07
Category : Technology & Engineering
ISBN : 1402090161

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This book focuses on the practical aspects of particle size measurement: a major difference with existing books, which have a more theoretical approach. Of course, the emphasis still lies on the measurement techniques. For optimum application, their theoretical background is accompanied by quantitative quality aspects, limitations and problem identification. In addition the book covers the phenomena of sampling and dispersion of powders, either of which may be dominant in the overall analysis error. Moreover, there are chapters on the general aspects of quality for particle size analysis, quality management, reference materials and written standards, in- and on-line measurement, definitions and multilingual terminology, and on the statistics required for adequate interpretation of results. Importantly, a relation is made to product performance, both during processing as well as in final application. In view of its set-up, this book is well suited to support particle size measurement courses.

Author : Yong Sun
Publisher :
Page : 0 pages
File Size : 48,61 MB
Release : 2004
Category : Light
ISBN :

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Static light scattering (SLS) and dynamic light scattering (DLS) techniques are used to measure characteristics of particles in dispersion. SLS measures the dependence of the average scattered intensity I, on the scattering angle and is sensitive to spatial variations in the dielectric constant E. DLS measures the time dependence of the scattered light. One fundamental application of light scattering techniques is the accurate measurement of the size distribution of particles in dispersion. Detailed experimental investigation of SLS and DLS has been attempted in this work, with experimental work based on dilute water dispersions of two different spherical particles, polystyrene latexes and poly(N-isopropylacrylamide) (PNIPAM) microgels. Size information is obtained from SLS measurements in the form of a particle size distribution G (R,) where R, is the static radius. Size information is obtained from DLS measurements in the form of a decay rate distribution G (I?) which depends on the decay rate I?. Although both SLS and DLS can be used to obtain size information from the scattered light, the information obtained using SLS and DLS is different. For the three polystyrene latex sphere samples studied in this thesis, the mean static radii obtained are consistent with that of the mean radii provided by the supplier. For all three samples, the apparent hydrodynamic radius is larger than the mean static radius by about 12%. For PNIPAM microgel spheres, the apparent hydrodynamic radius is also larger than the mean static radius. The size of the PNIPAM microgel particles is extremely temperature sensitive; the radius decreases by a factor of three as the temperature is raised from 15OC to 50?? Both the hydrodynamic and static radii show this behavior. The effect of the chemical crosslinker (N, N'-methylenebisacrylamide) content on the temperature sensitivity of the PNIPAM microgels and the temperature dependence of the ratio of the apparent hydrodynamic radius to the mean static radius are also discussed.

Author : N G Stanley-Wood
Publisher : Royal Society of Chemistry
Page : 557 pages
File Size : 38,77 MB
Release : 2007-10-31
Category : Science
ISBN : 1847551629

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Particle Size Analysis reviews the development of particle characterization over the past 25 years and also speculates on its future. Interest in the subject has increased enormously over the years and this book highlights the changes and advances made within the field. This book is comprehensive in its coverage of particle size analysis and includes contributions on such characterization techniques as microscopy using fractal analysis, light diffraction, light scattering with the phase doppler technique, light observation, and photon correlation spectroscopy. A number of chapters address the interest in on-line in-stream particle size analysis and illustrate the progress being made in achieving this long sought after ideal of in-situ in-process particle characterization. Applications to other technological fields are detailed by chapters covering biological systems and the pharmaceutical industry. The subject of surface area determination is considered with particular emphasis on the measurements on porosity of powders, the characterization and comparability of reference materials, and the need for standards. Particle Size Analysis should provide stimulating reading for technologists, scientists, and engineers involved in particle characterization and powder technology worldwide.

Author : Renliang Xu
Publisher : Springer Science & Business Media
Page : 411 pages
File Size : 25,9 MB
Release : 2006-04-11
Category : Science
ISBN : 0306471248

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Particle characterization is an important component in product research and development, manufacture, and quality control of particulate materials and an important tool in the frontier of sciences, such as in biotechnology and nanotechnology. This book systematically describes one major branch of modern particle characterization technology - the light scattering methods. This is the first monograph in particle science and technology covering the principles, instrumentation, data interpretation, applications, and latest experimental development in laser diffraction, optical particle counting, photon correlation spectroscopy, and electrophoretic light scattering. In addition, a summary of all major particle sizing and other characterization methods, basic statistics and sample preparation techniques used in particle characterization, as well as almost 500 latest references are provided. The book is a must for industrial users of light scattering techniques characterizing a variety of particulate systems and for undergraduate or graduate students who want to learn how to use light scattering to study particular materials, in chemical engineering, material sciences, physical chemistry and other related fields.

Author : T. Allen
Publisher : Elsevier
Page : 683 pages
File Size : 41,54 MB
Release : 2003-12-09
Category : Technology & Engineering
ISBN : 0080539327

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Powder technology is a rapidly expanding technology and nowhere more than in particle characterization. There has been an explosion of new particle measuring techniques in the past ten year particularly in the field of on-line measurement. One of the main aims of this book is to bring the reader up-to-date with current practices. One important area of interest is the improvements in on-line light scattering instruments and the introduction of ultrasonic on-line devices. Another is the introduction of on-line microscopy, which permits shape analysis in conjunction with particle sizing.Schools of powder technology are common in Europe and Japan but the importance of this subject has only recently been recognised in America with the emergence of the Particle Research Centre (PERC) at the University of Florida in Gainsville. - Details all the latest developments in powder technology - Written by established authority on powder technology- A comprehensive text covering all aspects of powder technology and handling of particulate solids including characterization, handling and applications

Author : Organización Internacional de Normalización
Publisher :
Page : 59 pages
File Size : 10,4 MB
Release : 2020
Category :
ISBN :

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This document provides guidance on instrument qualification and size distribution measurement of particles in many two-phase systems (e.g. powders, sprays, aerosols, suspensions, emulsions and gas bubbles in liquids) through the analysis of their light-scattering properties. It does not address the specific requirements of particle size measurement of specific materials.This document is applicable to particle sizes ranging from approximately 0,1 μm to 3 mm. With special instrumentation and conditions, the applicable size range can be extended above 3 mm and below 0,1 μm.For spherical and non-spherical particles, a size distribution is reported, where the predicted scattering pattern for the volumetric sum of spherical particles matches the measured scattering pattern. This is because the technique assumes a spherical particle shape in its optical model. For non-spherical particles the resulting particle size distribution is different from that obtained by methods based on other physical principles (e.g. sedimentation, sieving).

Author : Miroslaw Jonasz
Publisher : Elsevier
Page : 715 pages
File Size : 17,76 MB
Release : 2011-08-29
Category : Science
ISBN : 0080548679

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Light scattering-based methods are used to characterize small particles suspended in water in a wide range of disciplines ranging from oceanography, through medicine, to industry. The scope and accuracy of these methods steadily increases with the progress in light scattering research. This book focuses on the theoretical and experimental foundations of the study and modeling of light scattering by particles in water and critically evaluates the key constraints of light scattering models. It begins with a brief review of the relevant theoretical fundamentals of the interaction of light with condensed matter, followed by an extended discussion of the basic optical properties of pure water and seawater and the physical principles that explain them. The book continues with a discussion of key optical features of the pure water/seawater and the most common components of natural waters. In order to clarify and put in focus some of the basic physical principles and most important features of the experimental data on light scattering by particles in water, the authors employ simple models. The book concludes with extensive critical reviews of the experimental constraints of light scattering models: results of measurements of light scattering and of the key properties of the particles: size distribution, refractive index (composition), structure, and shape. These reviews guide the reader through literature scattered among more than 210 scientific journals and periodicals which represent a wide range of disciplines. A special emphasis is put on the methods of measuring both light scattering and the relevant properties of the particles, because principles of these methods may affect interpretation and applicability of the results. The book includes extensive guides to literature on light scattering data and instrumentation design, as well as on the data for size distributions, refractive indices, and shapes typical of particles in natural waters. It also features a comprehensive index, numerous cross-references, and a reference list with over 1370 entries. An errata sheet for this work can be found at: http://www.tpdsci.com/Ref/Jonasz_M_2007_LightScatE.php *Extensive reference section provides handy compilations of knowledge on the designs of light scattering meters, sources of experimental data, and more *Worked exercises and examples throughout